[1] |
国家药典委员会.中华人民共和国药典2015年版四部[S].北京:中国医药科技出版社,2015:441. |
[2] |
The United States Pharmacopeial Convention.U.S.Pharmacopeia 40-National Formulaty 35[S].The United States Pharmacopeial Convention.2017:761. |
[3] |
European Directorate for the Quality of Medicines & HealthCare.European Pharmacopoecia 9.0 Index[S].EDQM 2017:54. |
[4] |
WEBSTER G K,KUMAR S.Expanding the analytical toolbox:pharmaceutical application of quantitative NMR[J].Anal Chem,2014,86(23):11474-11480. |
[5] |
PAULI G F,CHEN S N,SIMMLER C,et al.Importance of purity evaluation and the potential of quantitative 1H NMR as a purity assay[J].J Med Chem,2014,57(22):9220-9231. |
[6] |
HOLZGRABE U,MALET-MARTINO M.Analytical challenges in drug counterfeiting and falsification-The NMR approach[J].J Pharm Biomed Anal,2011,55(4):679-687. |
[7] |
SANTOS PIMENTA L P,SCHILTHUIZEN M,VERPOORTE R,et al.Quantitative analysis of amygdalin and prunasin in Prunus serotina Ehrh.using 1H-NMR spectroscopy[J].Phytochem Anal,2014,25(2):122-126. |
[8] |
WEBER M,HELLRIEGEL C,RÜCK A,et al.Using high-performance quantitative NMR (HP-qNMR®) for certifying traceable and highly accurate purity values of organic reference materials with uncertainties <0.1%[J].Accred Qual Assur,2013,18(2):91-98. |
[9] |
BEKIROGLU S,MYRBERG O,OSTMAN K,et al.Validation of a quantitative NMR method for suspected counterfeit products exemplified on determination of benzethonium chloride in grapefruit seed extracts[J].J Pharm Biomed Anal,2008,47(4-5):958-961. |
[10] |
吴迪,陈华,王腾,等.19F核磁共振定量法测定吉非替尼的含量[J].中国新药杂志,2017,26(19):2343-2346. |
[11] |
李宏伟,张红芹,郝海军.核磁共振定量法测定恩曲他滨绝对含量[J].化学试剂,2018,40(8):755~758. |
[12] |
ZHANG FF,JIANG M H,SUN L L,et al.Quantitative analysis of sitagliptin using the 19F-NMR method:a universal technique for fluorinated compound detection[J].Analyst,2015,140(1):280-286. |
[13] |
DO N M,OLIVIER M A,SALISBURY JJ,et al.Application of quantitative 19F and 1H NMR for reaction monitoring and in situ yield determinations for an early stage pharmaceutical candidate[J].Anal Chem,2011,83(22):8766-8771. |
[14] |
张卫国,殷忠,郭华,等.用氟离子选择电极测定牙膏中游离氟的影响因素[J].中国地方病学杂志,2007,26(6):693-694. |