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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2015  >  33(1): 55-57

DING Huamin, GUO Yuchen, QIN Chunxia, SONG Zhibing, SUN Lili. Therapeutic effect of Xiaofeng Zhiyang granules on acute itching in mice with atopic dermatitis by decreasing leukotriene[J]. Journal of Pharmaceutical Practice and Service, 2024, 42(5): 211-216. doi: 10.12206/j.issn.2097-2024.202306031
Citation: CHANG Mingquan, CHEN Lin, HE Xiuli, CHEN Fang. Determination of dexamethasone acetate in Kelaweiding liniment by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(1): 55-57. doi: 10.3969/j.issn.1006-0111.2015.01.014
shu

Determination of dexamethasone acetate in Kelaweiding liniment by HPLC

doi: 10.3969/j.issn.1006-0111.2015.01.014

  • Taihe Hospital Affiliated to Hubei Medical College, Shiyan 442000, China

  • Received Date: 2014-01-24
  • Rev Recd Date: 2014-05-23
  • Objective To establish the quantitative determination method of dexamethasone acetate in Kelaweiding liniment by HPLC. Methods Column:Diamonsil-C18(150 mm×4.6 mm,5 μm),mobile phase:methanol-water-glacialaceticacid (80:20:0.5),flow rate:1.0 ml/min,UV detection wavelength:240 nm,injection volume :20 μl,column temperature:30℃. Results The standard curve was linear within the range of 2.00-64.00 μg/ml,linear equation was Y=0.405 2X+0.804 2(r=0.999 9).The average recovery was 99.3% with RSD 0.93% (n=9). Conclusion This method was simple,stable and could be used to assay dexamethasone acetate in Kelaweiding liniment.
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    [8] 陈 芳,常明泉,杜士明,等.不同浓度蒽酮-硫酸试液对白及溶胶含量的影响[J].中国药师,2012,15(11):1604-1605.
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Determination of dexamethasone acetate in Kelaweiding liniment by HPLC

doi: 10.3969/j.issn.1006-0111.2015.01.014
  • Taihe Hospital Affiliated to Hubei Medical College, Shiyan 442000, China
  • Received Date: 2014-01-24
  • Rev Recd Date: 2014-05-23

Abstract: Objective To establish the quantitative determination method of dexamethasone acetate in Kelaweiding liniment by HPLC. Methods Column:Diamonsil-C18(150 mm×4.6 mm,5 μm),mobile phase:methanol-water-glacialaceticacid (80:20:0.5),flow rate:1.0 ml/min,UV detection wavelength:240 nm,injection volume :20 μl,column temperature:30℃. Results The standard curve was linear within the range of 2.00-64.00 μg/ml,linear equation was Y=0.405 2X+0.804 2(r=0.999 9).The average recovery was 99.3% with RSD 0.93% (n=9). Conclusion This method was simple,stable and could be used to assay dexamethasone acetate in Kelaweiding liniment.

DING Huamin, GUO Yuchen, QIN Chunxia, SONG Zhibing, SUN Lili. Therapeutic effect of Xiaofeng Zhiyang granules on acute itching in mice with atopic dermatitis by decreasing leukotriene[J]. Journal of Pharmaceutical Practice and Service, 2024, 42(5): 211-216. doi: 10.12206/j.issn.2097-2024.202306031
Citation: CHANG Mingquan, CHEN Lin, HE Xiuli, CHEN Fang. Determination of dexamethasone acetate in Kelaweiding liniment by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(1): 55-57. doi: 10.3969/j.issn.1006-0111.2015.01.014
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