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Volume 33 Issue 3
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2015  >  33(3): 213-216

ZHANG Guoqing, LI Dan, WANG Kebing. Rapid identification of dye adulteration in Kadsura longipedunculata by paper-based SERS[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(3): 213-216. doi: 10.3969/j.issn.1006-0111.2015.03.006
Citation: ZHANG Guoqing, LI Dan, WANG Kebing. Rapid identification of dye adulteration in Kadsura longipedunculata by paper-based SERS[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(3): 213-216. doi: 10.3969/j.issn.1006-0111.2015.03.006
shu

Rapid identification of dye adulteration in Kadsura longipedunculata by paper-based SERS

doi: 10.3969/j.issn.1006-0111.2015.03.006
  • 1.

    Department of Pharmacy, No. 169 Hospital of PLA, Hengyang 421002, China

  • 2.

    School of Pharmacy, Second Military Medical University, Shanghai 200433, China

  • Received Date: 2015-02-13
  • Rev Recd Date: 2015-04-14
  • Objective To establish a paper-based surface-enhanced Raman scattering (SERS) method for the detection of dyed Kadsura longipedunculata Finet et Gagnep. Methods Supported silver nanoparticles on filter paper were synthesized simply by soaking method.In addition, factors including enrichment ratio of silver nanoparticles, the enhancement effect and stability of the SERS device were investigated. Results The Kadsura longipedunculata Finet et Gagnep, dyed by Erythrosine or Acid Red at low concentration had been detected successfully. Conclusion Combined with the paper device and SERS, the approach was rapid and non-destructive which could be used to identification of dyed Kadsura longipedunculata Finet et Gagnep.
  • [1] 国家药典委员会.中华人民共和国药典2010年版一部[S].北京:中国医药科技出版社, 2010: 227-228.
    [2] 汪 平,邬芙蓉, 成 龙. 五味子中掺伪品南五味子的鉴别[J]. 中国药业, 2004, 13(2): 62-63.
    [3] 魏 清, 魏俊德, 康红英. 南五味子中非法添加染料胭脂红赤藓红和酸性红 73 快速鉴别法[J]. 湖北中医药大学学报, 2013, 15(5): 38-40.
    [4] 孙 晶, 王 坤, 习超鹏,等. 几种中药材中添加人工合成色素的研究[J]. 中国药事, 2011, 25(12): 1200-1202.
    [5] 黄海欣. 77 批五味子的质量考察[J]. 中国药事, 2010, 24(12): 1228-1229.
    [6] Brosseau CL, Rayner KS, Casadio F, et al. Surface-enhanced Raman spectroscopy: a direct method to identify colorants in various artist media[J]. Anal Chem, 2009, 81(17):7443-7447.
    [7] Bruni S, Guglielmi V, Pozzi F,et al. Surface-enhanced Raman spectroscopy (SERS) on silver colloids for the identification of ancient textile dyes. Part II: pomegranate and sumac[J]. J Raman Spectrosc, 2011,42: 465-473.
    [8] Casadio F, Leona M, Lombardi JR,et al. Identification of organic colorants in fibers, paints, and glazes by surface enhanced Raman spectroscopy[J]. Acc Chem Res, 2010,43(6):782-791.
    [9] Zhu Q, Cao Y, Cao Y, et al. Rapid on-site TLC-SERS detection of four antidiabetes drugs used as adulterants in botanical dietary supplements[J]. Anal Bioanal Chem, 2014, 406(7): 1877-1884.
    [10] 尹利辉, 张 雁. 正电性纳米银胶的表征及加入不同凝聚剂后的表面增强拉曼散射光谱[J]. 药物分析杂志, 2010, 30(12): 2352-2355.
    [11] Kerker M, Siiman O, Wang DS. Effect of aggregates on extinction and surface-enhanced Raman scattering spectra of colloidal silver[J].J Phys Chem, 1984, 88(15): 3168-3170.
    [12] 黄 茜, 王 京, 曹丽冉, 等. 纳米 Ag 材料表面等离子体激元引起的表面增强拉曼散射光谱研究[J]. 物理学报, 2009, 58(3): 1980-1986.
    [13] Moskovits M. Persistent misconceptions regarding SERS[J]. Phys Chem Chem Phys, 2012, 15:5301-5311.
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Rapid identification of dye adulteration in Kadsura longipedunculata by paper-based SERS

doi: 10.3969/j.issn.1006-0111.2015.03.006
  • 1. Department of Pharmacy, No. 169 Hospital of PLA, Hengyang 421002, China
  • 2. School of Pharmacy, Second Military Medical University, Shanghai 200433, China
  • Received Date: 2015-02-13
  • Rev Recd Date: 2015-04-14

Abstract: Objective To establish a paper-based surface-enhanced Raman scattering (SERS) method for the detection of dyed Kadsura longipedunculata Finet et Gagnep. Methods Supported silver nanoparticles on filter paper were synthesized simply by soaking method.In addition, factors including enrichment ratio of silver nanoparticles, the enhancement effect and stability of the SERS device were investigated. Results The Kadsura longipedunculata Finet et Gagnep, dyed by Erythrosine or Acid Red at low concentration had been detected successfully. Conclusion Combined with the paper device and SERS, the approach was rapid and non-destructive which could be used to identification of dyed Kadsura longipedunculata Finet et Gagnep.

ZHANG Guoqing, LI Dan, WANG Kebing. Rapid identification of dye adulteration in Kadsura longipedunculata by paper-based SERS[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(3): 213-216. doi: 10.3969/j.issn.1006-0111.2015.03.006
Citation: ZHANG Guoqing, LI Dan, WANG Kebing. Rapid identification of dye adulteration in Kadsura longipedunculata by paper-based SERS[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(3): 213-216. doi: 10.3969/j.issn.1006-0111.2015.03.006
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