Message Board

Respected readers, authors and reviewers, you can add comments to this page on any questions about the contribution, review,        editing and publication of this journal. We will give you an answer as soon as possible. Thank you for your support!

Name
E-mail
Phone
Title
Content
Verification Code
x Close Forever Close
Volume 34 Issue 1
. 
Turn off MathJax
Article Contents
Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2016  >  34(1): 52-55

LI Ling, LÜ Lei, DONG Xin, LÜ Diya, XU Li. Analysis of volatile components from Actinidia valvata by HS-GC-MS based on retention index[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 52-55. doi: 10.3969/j.issn.1006-0111.2016.01.014
Citation: LI Ling, LÜ Lei, DONG Xin, LÜ Diya, XU Li. Analysis of volatile components from Actinidia valvata by HS-GC-MS based on retention index[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 52-55. doi: 10.3969/j.issn.1006-0111.2016.01.014
shu

Analysis of volatile components from Actinidia valvata by HS-GC-MS based on retention index

doi: 10.3969/j.issn.1006-0111.2016.01.014
  • 1.

    Pharmaceutical Analysis Center, School of Pharmacy, Second Military Medical University of PLA, Shanghai 200433, China

  • 2.

    Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China

  • 3.

    Department of Medicinal Instrument, No.113 Hospital of PLA, Ningbo 315040, China

  • Received Date: 2014-10-29
  • Rev Recd Date: 2015-03-08
  • Objective To establish a method for determining volatile components from Actinidia valvata Dunn. Methods A static headspace-gas chromatography-mass spectrometry (HS-GC-MS) method was used to analyze volatile components,and the separated peaks were identified by mass spectal library searching combined with retention index comparison. Results 42 volatile components were separated from Actinidia valvata Dunn and 25 of them were identified,mainly including alcohols,esters,aldehydes,hydrocarbons and so on. Conclusion Combined with retention index calculation,this method improved accuracy of qualitation of HS-GC-MS and provided scientific proof for the exploitation and utilization of Actinidia valvata Dunn.
  • [1] 陈 豪,潘坤官,何丽君. 抗癌中药猫人参研究概况[J]. 海峡药学,2011,23(12):9-11.
    [2] 徐一新, 项昭保, 陈晓晶, 等. 中药猫人参中的抗肿瘤活性成分[J]. 第二军医大学学报, 2011, 32(7):749-753.
    [3] Federica B,Maria C,Alessandro M,et al.Retention indices in the analysis of food aroma volatile compounds in temperature programmed gas chromatography:database creation and evaluation of precision and robustness[J].J Sep Sci,2007,30(4):563-572.
    [4] 李浩春. 分析化学手册[M]. 2版. 北京: 化学工业出版社, 1999:46.
    [5] Vanden D,Kratz PD.A generalization of the retention index system including linear temperature programmed gas-liquid partition chromatography[J]. J Chromatogr, 1963, 11: 463-471.
    [6] 梁 晟,李雅文,赵晨曦,等. GC-MS结合保留指数对中药挥发油的定性[J]. 分析测试学报,2008, 27(1): 84-87.
    [7] 王 坚,陈鸿平,刘友平,等. Kováts保留指数在中药挥发油成分定性中的作用-青皮[J]. 中国实验方剂学杂志,2013,19(14):92-96.
    [8] 陈 艳. 肉豆蔻精油挥发性组分色谱保留指数的预测[J]. 食品科学, 2011, 32(12):274-277.
    [9] 辛海量, 徐燕丰, 吴迎春, 等. 猫人参化学成分的气相色谱-质谱联用分析[J]. 时珍国医国药, 2009,20(6): 1299-1300.
    [10] 袁 珂,朱建鑫,张 耀,等. 猫人参化学成分研究[J]. 中草药,2008,39(4):505-507.
    [11] 丁丽丽,王顺春,王峥涛. 猫人参化学成分的研究[J]. 中国中药杂志,2007,32(18):1893-1895.
    [12] 谢显珍, 王玉林, 朱丹晖, 等. 气相色谱-质谱联用结合保留指数分析仙鹤草挥发性成分[J]. 分析科学学报,2013,29(5): 651-654.
    [13] 刘永波,赵慎晃,薛瑞芳. 顶空-气相色谱-质谱联用法测定水和废水中8种苯系物[J]. 环境监测管理与技术,2012,24(1): 43-46.
    [14] 苏 越,姬厚伟,苏式兵,等. GC-MS中保留指数和保留温度回归分析应用于单萜烯结构确认[J]. 分析测试技术与仪器,2008,14(3): 131-135.
    [15] 苏 越,刘素红,王呈仲,等. 谱图相似度分析结合保留指数对单萜烯同分异构体的GC-MS定性分析[J]. 分析测试学报,2009,28(5): 525-528.
  • 加载中
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Get Citation
PDF
XML

Article Metrics

Article views(3200) PDF downloads(102) Cited by()

Related
Proportional views

Analysis of volatile components from Actinidia valvata by HS-GC-MS based on retention index

doi: 10.3969/j.issn.1006-0111.2016.01.014
  • 1. Pharmaceutical Analysis Center, School of Pharmacy, Second Military Medical University of PLA, Shanghai 200433, China
  • 2. Department of Pharmacy, Eastern Hepatobiliary Surgery Hospital, Shanghai 200438, China
  • 3. Department of Medicinal Instrument, No.113 Hospital of PLA, Ningbo 315040, China
  • Received Date: 2014-10-29
  • Rev Recd Date: 2015-03-08

Abstract: Objective To establish a method for determining volatile components from Actinidia valvata Dunn. Methods A static headspace-gas chromatography-mass spectrometry (HS-GC-MS) method was used to analyze volatile components,and the separated peaks were identified by mass spectal library searching combined with retention index comparison. Results 42 volatile components were separated from Actinidia valvata Dunn and 25 of them were identified,mainly including alcohols,esters,aldehydes,hydrocarbons and so on. Conclusion Combined with retention index calculation,this method improved accuracy of qualitation of HS-GC-MS and provided scientific proof for the exploitation and utilization of Actinidia valvata Dunn.

LI Ling, LÜ Lei, DONG Xin, LÜ Diya, XU Li. Analysis of volatile components from Actinidia valvata by HS-GC-MS based on retention index[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 52-55. doi: 10.3969/j.issn.1006-0111.2016.01.014
Citation: LI Ling, LÜ Lei, DONG Xin, LÜ Diya, XU Li. Analysis of volatile components from Actinidia valvata by HS-GC-MS based on retention index[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(1): 52-55. doi: 10.3969/j.issn.1006-0111.2016.01.014
shu

    HTML

Reference (15)

Catalog

    版权所有：《药学实践与服务》编辑委员会

    Supervisor & Sponsors: Address: No 325 Guohe Road, ShanghaiPost Code: 200433

    Tel: （021）81871324,81871397 E-mail: yxsjzzs@163.com

    网站备案号 沪ICP备05003363号-1

    Supported by: Beijing Renhe Information Technology Co., Ltd.  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return