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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2017  >  35(3): 256-258

TAO Xiaoxuan, LI Gang, XU Lan, ZHANG Qiang. Study on quality standard of Compound Belladonna Mixture[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(3): 256-258. doi: 10.3969/j.issn.1006-0111.2017.03.015
Citation: TAO Xiaoxuan, LI Gang, XU Lan, ZHANG Qiang. Study on quality standard of Compound Belladonna Mixture[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(3): 256-258. doi: 10.3969/j.issn.1006-0111.2017.03.015
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Study on quality standard of Compound Belladonna Mixture

doi: 10.3969/j.issn.1006-0111.2017.03.015

  • Department of Phamacy, No.94 Hospital of PLA, Nanchang 330002, China

  • Received Date: 2015-02-15
  • Rev Recd Date: 2015-08-03
  • Objective To improve the quality standard for Compound Belladonna Mixture. Methods TLC was used for the qualitative identification of morphine. HPLC was used for the content of morphine in the Compound Belladonna Mixture. Results Morphine could be identified by TLC. A good linear correlation of morphine was observed within the range of 0.525~10.5 μg/ml (r= 0.999 9).The average recovery was 99.44% with RSD of 0.23% (n=9). Conclusion This method is simple,accurate and quick, which could be used for determination and quality control of Compound Belladonna Mixture with good selectivity and repeatability.
  • [1] 中国人民解放军总后勤卫生部.中国人民解放军医疗机构制剂规范[S].北京:人民军医出版社,2002:33.
    [2] 汤方萍,杨立香.高效液相色谱法测定复方樟脑酊中吗啡含量[J].中国医院药学杂志,2008,28(14);1227-1228.
    [3] 国家药典委员会.中华人民共和国药典2010年版二部[S].北京:中国医药科技出版社,2010:593-594.
    [4] 熊水莲,侯 莉. 固相萃取柱高效液相色谱法测定复方甘草含片中吗啡的含量[J].实用临床医学,2012,13(10):10-12.
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Study on quality standard of Compound Belladonna Mixture

doi: 10.3969/j.issn.1006-0111.2017.03.015
  • Department of Phamacy, No.94 Hospital of PLA, Nanchang 330002, China
  • Received Date: 2015-02-15
  • Rev Recd Date: 2015-08-03

Abstract: Objective To improve the quality standard for Compound Belladonna Mixture. Methods TLC was used for the qualitative identification of morphine. HPLC was used for the content of morphine in the Compound Belladonna Mixture. Results Morphine could be identified by TLC. A good linear correlation of morphine was observed within the range of 0.525~10.5 μg/ml (r= 0.999 9).The average recovery was 99.44% with RSD of 0.23% (n=9). Conclusion This method is simple,accurate and quick, which could be used for determination and quality control of Compound Belladonna Mixture with good selectivity and repeatability.

TAO Xiaoxuan, LI Gang, XU Lan, ZHANG Qiang. Study on quality standard of Compound Belladonna Mixture[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(3): 256-258. doi: 10.3969/j.issn.1006-0111.2017.03.015
Citation: TAO Xiaoxuan, LI Gang, XU Lan, ZHANG Qiang. Study on quality standard of Compound Belladonna Mixture[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(3): 256-258. doi: 10.3969/j.issn.1006-0111.2017.03.015
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