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Volume 36 Issue 4
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2018  >  36(4): 343-346

CAO Hong, SHAN Tingting, HU Dan, ZHANG Guiying. Study on the quality standard for Fenghan Shiling San[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(4): 343-346. doi: 10.3969/j.issn.1006-0111.2018.04.012
Citation: CAO Hong, SHAN Tingting, HU Dan, ZHANG Guiying. Study on the quality standard for Fenghan Shiling San[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(4): 343-346. doi: 10.3969/j.issn.1006-0111.2018.04.012
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Study on the quality standard for Fenghan Shiling San

doi: 10.3969/j.issn.1006-0111.2018.04.012

  • The Institute for Drug and Instrument Control of Directorate of Medical Services and Logistics Support, Central Military Commission of PRC, Beijing 100071, China

  • Received Date: 2017-11-28
  • Rev Recd Date: 2018-01-09
  • Objective To revise and improve the quality standard for Fenghan Shiling San. Methods The thin layer chromatography was used to identify euphorbiae ebracteolatae radix, angelicae dahuricae radix, notoginseng radix et rhizome, radix paeoniae rubra and rhizoma curcumae longae. The high-performance liquid chromatography was applied to determine the contents of imperatorin in Fenghan Shiling San. Results Euphorbiae ebracteolatae radix, angelicae dahuricae radix, notoginseng radix et rhizome, radix paeoniae rubra and rhizoma curcumae longae can be identified by TLC. Imperatorin showed a good linear relationship in a range of 0.033 6-0.269 0 μg, r=0.999 9. The average recovery of imperatorin was 96.77%(RSD=1.63%, n=6). Conclusion This accurate and quick method can be used for the quality control of Fenghan Shiling San.
  • [1] 国家药典委员会.中华人民共和国药典(一部,四部):2015年版[S].北京:化学工业出版社,2015:11,105,158,264,286,通则0502.
    [2] 彭春梅,赵英.高效液相色谱法测定清眩丸中欧前胡素含量[J].中国药业,2014,23(3):35-36.
    [3] 曹红,邢俊波,陈玉敏,等.都梁丸质量标准的研究[J].解放军药学学报,2012,28(5):417-419.
    [4] 李思思,许浚,张铁军,等.HPLC法同时测定元胡止痛滴丸中6种成分[J].中草药,2015,46(21):3198-3201.
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Study on the quality standard for Fenghan Shiling San

doi: 10.3969/j.issn.1006-0111.2018.04.012
  • The Institute for Drug and Instrument Control of Directorate of Medical Services and Logistics Support, Central Military Commission of PRC, Beijing 100071, China
  • Received Date: 2017-11-28
  • Rev Recd Date: 2018-01-09

Abstract: Objective To revise and improve the quality standard for Fenghan Shiling San. Methods The thin layer chromatography was used to identify euphorbiae ebracteolatae radix, angelicae dahuricae radix, notoginseng radix et rhizome, radix paeoniae rubra and rhizoma curcumae longae. The high-performance liquid chromatography was applied to determine the contents of imperatorin in Fenghan Shiling San. Results Euphorbiae ebracteolatae radix, angelicae dahuricae radix, notoginseng radix et rhizome, radix paeoniae rubra and rhizoma curcumae longae can be identified by TLC. Imperatorin showed a good linear relationship in a range of 0.033 6-0.269 0 μg, r=0.999 9. The average recovery of imperatorin was 96.77%(RSD=1.63%, n=6). Conclusion This accurate and quick method can be used for the quality control of Fenghan Shiling San.

CAO Hong, SHAN Tingting, HU Dan, ZHANG Guiying. Study on the quality standard for Fenghan Shiling San[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(4): 343-346. doi: 10.3969/j.issn.1006-0111.2018.04.012
Citation: CAO Hong, SHAN Tingting, HU Dan, ZHANG Guiying. Study on the quality standard for Fenghan Shiling San[J]. Journal of Pharmaceutical Practice and Service, 2018, 36(4): 343-346. doi: 10.3969/j.issn.1006-0111.2018.04.012
shu

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