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Fang Hongzhuang, Lei Lili, Liu Xingbao. Determination of phenacetin and caffeine in compound acetylsalicylic acid tablets by multiple regression spectrophotometry[J]. Journal of Pharmaceutical Practice and Service, 1999, (1): 31-33.
Citation: Fang Hongzhuang, Lei Lili, Liu Xingbao. Determination of phenacetin and caffeine in compound acetylsalicylic acid tablets by multiple regression spectrophotometry[J]. Journal of Pharmaceutical Practice and Service, 1999, (1): 31-33.

Determination of phenacetin and caffeine in compound acetylsalicylic acid tablets by multiple regression spectrophotometry

  • Received Date: 1998-07-07
  • OBJECTIVE To determine phenacetin and caffeine in compound acetylsalicylic acid tablets. METHODS Multiple regression spectrophotometry was adopted as follow:The sample is dissolved in ethanol,add solution of 02mol/L NaOH to hydrolysis acetylsalicylic acid,the components are determined in phosphate salt buffet (pH 6.5). RESULTS The average recoveries for phenacetin and caffeine were 99.8% and 99.9%,with RSD 0.72% and 0.52%,respectively. CONCLUSION Accuracy of the method was compared with official quantitative analysis and no significant difference was found.
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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Determination of phenacetin and caffeine in compound acetylsalicylic acid tablets by multiple regression spectrophotometry

Abstract: OBJECTIVE To determine phenacetin and caffeine in compound acetylsalicylic acid tablets. METHODS Multiple regression spectrophotometry was adopted as follow:The sample is dissolved in ethanol,add solution of 02mol/L NaOH to hydrolysis acetylsalicylic acid,the components are determined in phosphate salt buffet (pH 6.5). RESULTS The average recoveries for phenacetin and caffeine were 99.8% and 99.9%,with RSD 0.72% and 0.52%,respectively. CONCLUSION Accuracy of the method was compared with official quantitative analysis and no significant difference was found.

Fang Hongzhuang, Lei Lili, Liu Xingbao. Determination of phenacetin and caffeine in compound acetylsalicylic acid tablets by multiple regression spectrophotometry[J]. Journal of Pharmaceutical Practice and Service, 1999, (1): 31-33.
Citation: Fang Hongzhuang, Lei Lili, Liu Xingbao. Determination of phenacetin and caffeine in compound acetylsalicylic acid tablets by multiple regression spectrophotometry[J]. Journal of Pharmaceutical Practice and Service, 1999, (1): 31-33.

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