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Volume 26 Issue 1
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2008  >  (1): 51-53

SU Ming-wu, LIU Jun, YAO Xue-lian, YUAN Zheng, YIN Jiu. Determination of bergeninum in Yinxian Tongfeibao granules by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (1): 51-53.
Citation: SU Ming-wu, LIU Jun, YAO Xue-lian, YUAN Zheng, YIN Jiu. Determination of bergeninum in Yinxian Tongfeibao granules by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (1): 51-53.
shu

Determination of bergeninum in Yinxian Tongfeibao granules by HPLC

  • 1.

    Hubei College of Traditional Chinese Medicine,Wuhan 430061,China

  • 2.

    Jiangxi College of Traditional Chinese Medicine,Nanchang 330000,China

  • Received Date: 2006-04-24
  • Rev Recd Date: 2006-08-28
  • Objective: To develop a HPLC method for determining bergeninum in Yinxian Tongfeibao granules. Methods: Zorbax Eclipse XDB-C18 column was used and methanol-water-acetic acid glacial（18-81-1） was used as mobil phase,detection wavelegth was 275 nm,the flow rate was 0.8 mL/min,column temperature was 30 ℃. Results: There was a good linear relationship in the range of 0.43-2.15 μg, r=0.999 88.The average recovery was 98.33% with RSD=2.68%. Conclusion: The method is rapid ,accurate and repeatable.It can be applied to an effective control of the quantity of Yinxian Tongfeibao granules.
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  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

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Determination of bergeninum in Yinxian Tongfeibao granules by HPLC

  • 1. Hubei College of Traditional Chinese Medicine,Wuhan 430061,China
  • 2. Jiangxi College of Traditional Chinese Medicine,Nanchang 330000,China
  • Received Date: 2006-04-24
  • Rev Recd Date: 2006-08-28

Abstract: Objective: To develop a HPLC method for determining bergeninum in Yinxian Tongfeibao granules. Methods: Zorbax Eclipse XDB-C18 column was used and methanol-water-acetic acid glacial（18-81-1） was used as mobil phase,detection wavelegth was 275 nm,the flow rate was 0.8 mL/min,column temperature was 30 ℃. Results: There was a good linear relationship in the range of 0.43-2.15 μg, r=0.999 88.The average recovery was 98.33% with RSD=2.68%. Conclusion: The method is rapid ,accurate and repeatable.It can be applied to an effective control of the quantity of Yinxian Tongfeibao granules.

SU Ming-wu, LIU Jun, YAO Xue-lian, YUAN Zheng, YIN Jiu. Determination of bergeninum in Yinxian Tongfeibao granules by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (1): 51-53.
Citation: SU Ming-wu, LIU Jun, YAO Xue-lian, YUAN Zheng, YIN Jiu. Determination of bergeninum in Yinxian Tongfeibao granules by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (1): 51-53.
shu

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