Message Board

Respected readers, authors and reviewers, you can add comments to this page on any questions about the contribution, review,        editing and publication of this journal. We will give you an answer as soon as possible. Thank you for your support!

Name
E-mail
Phone
Title
Content
Verification Code
x Close Forever Close
Volume 26 Issue 2
. 
Turn off MathJax
Article Contents
Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2008  >  (2): 143-145

XUE Ke-chang, SHI Ning, TAN Sheng-jian, CHI Jia-ping, JIANG Li, WU Jiu-hong. Determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (2): 143-145.
Citation: XUE Ke-chang, SHI Ning, TAN Sheng-jian, CHI Jia-ping, JIANG Li, WU Jiu-hong. Determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (2): 143-145.
shu

Determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets by HPLC

  • Department of Pharmacy,306th Hospital of PLA,Beijing 100101,China

  • Objective: To develop a HPLC quantitative method for the determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets. Methods: The chromatographic conditions include column C18(Agilent ZORBAX Eclipse XDB-C18,4.6×150 mm,5 μm),mobile phase:acetonitrile-water(55-45),flow rate 1.0 mL/min and detection wavelength 327 nm. Results: The regresstion equation of cryptotanshinone and tanshinone ⅡA was Y=0.000 270 9X+0.001 090,r=0.999 9,Y=0.000 255 6X+0.001 055,r=0.999 9.The linear range was 0.036 00～1.440 μg and 0.030 00～1.200 μg.The average recovery of cryptotanshinone and tanshinone ⅡA were 101.7%(RSD 0.28%),100.8%(RSD 0.50%)respectively. Conclusion: The method was sensitive,rapid and accurate.
  • 加载中
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Get Citation
PDF
XML

Article Metrics

Article views(2663) PDF downloads(521) Cited by()

Related
Proportional views

Determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets by HPLC

  • Department of Pharmacy,306th Hospital of PLA,Beijing 100101,China

Abstract: Objective: To develop a HPLC quantitative method for the determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets. Methods: The chromatographic conditions include column C18(Agilent ZORBAX Eclipse XDB-C18,4.6×150 mm,5 μm),mobile phase:acetonitrile-water(55-45),flow rate 1.0 mL/min and detection wavelength 327 nm. Results: The regresstion equation of cryptotanshinone and tanshinone ⅡA was Y=0.000 270 9X+0.001 090,r=0.999 9,Y=0.000 255 6X+0.001 055,r=0.999 9.The linear range was 0.036 00～1.440 μg and 0.030 00～1.200 μg.The average recovery of cryptotanshinone and tanshinone ⅡA were 101.7%(RSD 0.28%),100.8%(RSD 0.50%)respectively. Conclusion: The method was sensitive,rapid and accurate.

XUE Ke-chang, SHI Ning, TAN Sheng-jian, CHI Jia-ping, JIANG Li, WU Jiu-hong. Determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (2): 143-145.
Citation: XUE Ke-chang, SHI Ning, TAN Sheng-jian, CHI Jia-ping, JIANG Li, WU Jiu-hong. Determination of cryptotanshinone and tanshinone ⅡA in Danshentong buccal tablets by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2008, (2): 143-145.
shu

    HTML

Catalog

    版权所有：《药学实践与服务》编辑委员会

    Supervisor & Sponsors: Address: No 325 Guohe Road, ShanghaiPost Code: 200433

    Tel: （021）81871324,81871397 E-mail: yxsjzzs@163.com

    网站备案号 沪ICP备05003363号-1

    Supported by: Beijing Renhe Information Technology Co., Ltd.  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return