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Volume 27 Issue 4
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2009  >  27(4): 286-288

WANG Liang, NI Lan, ZHANG Chun-Mei, GUO Jun-Xiang, HU Hong-Gang, WU Qiu-Ye. Study on synthesis of Fmoc-L-Asp-4-OBn[J]. Journal of Pharmaceutical Practice and Service, 2011, 29(1): 27-28.
Citation: HUANG Hong-wen, TANG Li-li, TAN Xiao-yong, JIANG Lan-ying. Content determination of hyperoside for Shanzha Maiqu granule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2009, 27(4): 286-288.
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Content determination of hyperoside for Shanzha Maiqu granule by HPLC

  • Shaoguan Institute for Drug Control, Shaoguan 512028, China

  • Received Date: 2008-12-03
  • Objective :To establish a method for determination of hyperoside in Shanzha Maiqu granule. Methods :HPLC was adopted with Agilent ZORBAX SB-C18 column(4.6 mm×250 mm,5 μm),methanol-tetrahydrofuran-0.5% H3PO4(0.917.681.5) as mobile phase at flow rate of 1.0 mL/min and 360 nm as detecting wavelength.Column temperature was room temperature and sample size was 20 μL. Results :The linear range of hyperoside was 0.018 624～0.465 6 μg(r=0.999 9).The average recovery rate of hyperoside was 96.09% and RSD was 0.82%(n=5).The contents of hyperoside in ten batches of Shanzha Maiqu granule were deteminted between 49～65 μg. Conclusion :This method is simple,accurate and reproducible,suitable for quality control of the drug.
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Content determination of hyperoside for Shanzha Maiqu granule by HPLC

  • Shaoguan Institute for Drug Control, Shaoguan 512028, China
  • Received Date: 2008-12-03

Abstract: Objective :To establish a method for determination of hyperoside in Shanzha Maiqu granule. Methods :HPLC was adopted with Agilent ZORBAX SB-C18 column(4.6 mm×250 mm,5 μm),methanol-tetrahydrofuran-0.5% H3PO4(0.917.681.5) as mobile phase at flow rate of 1.0 mL/min and 360 nm as detecting wavelength.Column temperature was room temperature and sample size was 20 μL. Results :The linear range of hyperoside was 0.018 624～0.465 6 μg(r=0.999 9).The average recovery rate of hyperoside was 96.09% and RSD was 0.82%(n=5).The contents of hyperoside in ten batches of Shanzha Maiqu granule were deteminted between 49～65 μg. Conclusion :This method is simple,accurate and reproducible,suitable for quality control of the drug.

WANG Liang, NI Lan, ZHANG Chun-Mei, GUO Jun-Xiang, HU Hong-Gang, WU Qiu-Ye. Study on synthesis of Fmoc-L-Asp-4-OBn[J]. Journal of Pharmaceutical Practice and Service, 2011, 29(1): 27-28.
Citation: HUANG Hong-wen, TANG Li-li, TAN Xiao-yong, JIANG Lan-ying. Content determination of hyperoside for Shanzha Maiqu granule by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2009, 27(4): 286-288.
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