Message Board

Respected readers, authors and reviewers, you can add comments to this page on any questions about the contribution, review,        editing and publication of this journal. We will give you an answer as soon as possible. Thank you for your support!

Name
E-mail
Phone
Title
Content
Verification Code

LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.
Citation: LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.

Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC

  • Received Date: 2010-07-08
  • Rev Recd Date: 2010-09-09
  • Objective To establish a HPLC method for the determination of prim-O-glucosylcimifugin,cimifugin,4'-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhammaudol in Radix Saposhnikoviae. Methods The sample was analyzed on an Agilent Zorbax SB-C18(5 μm,150 mm×4.6 mm id) column with methanol-water mobile phase for the gradient elution.The detection wavelength was 254 nm and flow rate was 0.7 ml/min.The column temperature was 25 ℃ and injection volume was 5 μl. Results The HPLC method for the determination of four major components in Radix Saposhnikoviae was established.The result of method was good. Conclusion The method was simple and feasible,and accurate which could be available for the quality control of Radix Saposhnikoviae.
  • 加载中
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索

Article Metrics

Article views(3741) PDF downloads(1174) Cited by()

Related
Proportional views

Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC

Abstract: Objective To establish a HPLC method for the determination of prim-O-glucosylcimifugin,cimifugin,4'-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhammaudol in Radix Saposhnikoviae. Methods The sample was analyzed on an Agilent Zorbax SB-C18(5 μm,150 mm×4.6 mm id) column with methanol-water mobile phase for the gradient elution.The detection wavelength was 254 nm and flow rate was 0.7 ml/min.The column temperature was 25 ℃ and injection volume was 5 μl. Results The HPLC method for the determination of four major components in Radix Saposhnikoviae was established.The result of method was good. Conclusion The method was simple and feasible,and accurate which could be available for the quality control of Radix Saposhnikoviae.

LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.
Citation: LI Yue-yue, WANG Hui, CHEN Jun, ZHAO Liang, ZHANG Hai, ZHANG Guo-qing. Determination of prim-O-glucosylcimifugin,cimifugin,4′-O-glucosyl-5-O-methylvisamminol and sec-O-β-D-glucosylhamma-udol in Radix Saposhnikoviae by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(6): 445-447,474.

Catalog

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return