Study on HPLC fingerprint of Semen Sojae Preparatum(SSP)

LIAO Li-na; ZHANG Ming-min; CAO Wei-wei; MAO Jun-qin

doi:10.3969/j.issn.1006-0111.2012.05.009

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Volume 30 Issue 5

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Article Navigation > Journal of Pharmaceutical Practice and Service > 2012 > 30(5): 351-352,386

LIAO Li-na, ZHANG Ming-min, CAO Wei-wei, MAO Jun-qin. Study on HPLC fingerprint of Semen Sojae Preparatum(SSP)[J]. Journal of Pharmaceutical Practice and Service, 2012, 30(5): 351-352,386. doi: 10.3969/j.issn.1006-0111.2012.05.009

Citation:

LIAO Li-na, ZHANG Ming-min, CAO Wei-wei, MAO Jun-qin. Study on HPLC fingerprint of Semen Sojae Preparatum(SSP)[J]. Journal of Pharmaceutical Practice and Service, 2012, 30(5): 351-352,386. doi: 10.3969/j.issn.1006-0111.2012.05.009

Study on HPLC fingerprint of Semen Sojae Preparatum(SSP)

doi: 10.3969/j.issn.1006-0111.2012.05.009

1.
Anhui Institute of Traditional Chinese Medicine, Hefei 230038, China
2.
411st hospital of PLA, Shanghai 200433, China
3.
85th hospital of PLA, Shanghai 200053, China

Received Date: 2012-03-04
Rev Recd Date: 2012-05-09

Abstract

To establish a HPLC fingerprint method for Semen Sojae Preparatumto quality control. Methods HPLC analysis was performed on a Diamonsil C₁₈ column (250 mm×4.6 mm,5 μm),the mobile phase was used in gradient elution consisted of methanol-water(3% acetic acid),the flow rate was 1.0 ml /min, column temperature was 30℃ and UV detected was set at 261 nm,the sample weight:10 μl. Results The compound composition of different SSP origins was obviously comparable, which could be determined by HPLC fingerprint of the SSP. Conclusion This method could be utilized as a quality control measurement for SSP.
- SSP,
- high performance liquid chromatography (HPLC),
- high performance liquid chromatographic fingerprint (HPLC-FPS)

References

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通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

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