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Volume 31 Issue 5
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2013  >  31(5): 386-387

LUO Chen-qu, LV Qing-hua. Determination of 2,3,5,4'-stilbene glucoside in Yangxueanshen Pills by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2013, 31(5): 386-387. doi: 10.3969/j.issn.1006-0111.2013.05.020
Citation: LUO Chen-qu, LV Qing-hua. Determination of 2,3,5,4'-stilbene glucoside in Yangxueanshen Pills by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2013, 31(5): 386-387. doi: 10.3969/j.issn.1006-0111.2013.05.020
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Determination of 2,3,5,4'-stilbene glucoside in Yangxueanshen Pills by HPLC

doi: 10.3969/j.issn.1006-0111.2013.05.020

  • Loudi Institute for Drug control, Loudi 417000, China

  • Received Date: 2012-07-11
  • Rev Recd Date: 2012-12-10
  • Objective To establish a HPLC method for determination of stilbene glucoside in Yangxueanshen Pills. Methods The Waters C18 column (4.6 mm×250 mm, 5 μm) was used. The mobile phase was acetonitrile-water (20:80).The flow rate was 1.0 ml/min.The detection wavelength was 320 nm. Results The linear range was 0.086 7 μg~1.083 5 μg(r=0.999 8). The average recovery was 99.2% with RSD=1.1% (n=9). Conclusion The determination method was simple, accurate, sensitive and reproducible which could be used for quality control of Yangxueanshen Pills.
  • [1] 李 铮,傅欣彤,张小茜,等.养血安神丸质量标准研究[J].中国中医药信息杂志.2009,16(7):48.
    [2] 中国药典2010年版.一部[S].2010:249.
    [3] 封玉英,何世新,封海霞,等.高效液相色谱法测定养血安神片的含量[J].中国药业.2007,16(9):16.
    [4] 中国药典2010年版一部[S].2010:947.
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Determination of 2,3,5,4'-stilbene glucoside in Yangxueanshen Pills by HPLC

doi: 10.3969/j.issn.1006-0111.2013.05.020
  • Loudi Institute for Drug control, Loudi 417000, China
  • Received Date: 2012-07-11
  • Rev Recd Date: 2012-12-10

Abstract: Objective To establish a HPLC method for determination of stilbene glucoside in Yangxueanshen Pills. Methods The Waters C18 column (4.6 mm×250 mm, 5 μm) was used. The mobile phase was acetonitrile-water (20:80).The flow rate was 1.0 ml/min.The detection wavelength was 320 nm. Results The linear range was 0.086 7 μg~1.083 5 μg(r=0.999 8). The average recovery was 99.2% with RSD=1.1% (n=9). Conclusion The determination method was simple, accurate, sensitive and reproducible which could be used for quality control of Yangxueanshen Pills.

LUO Chen-qu, LV Qing-hua. Determination of 2,3,5,4'-stilbene glucoside in Yangxueanshen Pills by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2013, 31(5): 386-387. doi: 10.3969/j.issn.1006-0111.2013.05.020
Citation: LUO Chen-qu, LV Qing-hua. Determination of 2,3,5,4'-stilbene glucoside in Yangxueanshen Pills by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2013, 31(5): 386-387. doi: 10.3969/j.issn.1006-0111.2013.05.020
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