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Volume 32 Issue 5
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2014  >  32(5): 357-359

WANG Chongqing, MA Ningning, YANG Chao, LIU Shihao, ZHU Ju, ZHENG Canhui. Research progress in the catalytic rearrangement reaction of benzyl phenyl ethers[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(6): 486-489. doi: 10.3969/j.issn.1006-0111.2015.06.002
Citation: JIA Yanhua, XIONG Chengwen. Study on the identification of raceanisodamine tablets by near infrared spectroscopy[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(5): 357-359. doi: 10.3969/j.issn.1006-0111.2014.05.011
shu

Study on the identification of raceanisodamine tablets by near infrared spectroscopy

doi: 10.3969/j.issn.1006-0111.2014.05.011
  • 1.

    Department of Pharmacy, First Affiliated Hospital, General Hospital of PLA, Beijing 100048, China

  • 2.

    Qinghai Institute for Drug Control, Xining 810016, China

  • Received Date: 2013-12-30
  • Rev Recd Date: 2013-10-29
  • Objective To develop an identification model of raceanisodamine tablets by diffuse reflection near-infrared spectroscopy and pattern recognition. Methods The diffuse reflectance spectra in the 12 000-4 000 cm-1 spectral coverage range of raceanisodamine tablets from eight different pharmaceutical factories were collected to establish the identification model.A mono-component near infrared model was established for raceanisodamine tablets. Results The parameters of the identification model for the raceanisodamine tablets was as follows:spectral range was 5 400-7 000 cm-1, the pretreatment method was first derivative and normalization; the threshold was 0.603. And the model was validated, which met the requirements of application. Conclusion The results showed that identification model for the raceanisodamine tablets by near infrared spectroscopy was feasible, which provided a reference method for the model updating.
  • [1] 金 宏.山莨菪碱的药理和临床应用研究进展[J].求医问药,2012,10(6):800-801.
    [2] 国家药典委员会,中华人民共和国药典2010年版二部[S].北京:中国医药科技出版社, 2010:866-868.
    [3] 卜媛媛.HPLC法测定盐酸消旋山莨菪碱注射液含量[J].药物与临床,2010,5(5):76.
    [4] 丁 燕,修 虹.HPLC法测定盐酸消旋山莨菪碱注射液中主药的含量[J].中国药房,2009,20(7):540-541.
    [5] 金 鸣,胡 敏,池文杰,等.近红外漫反射光谱法快速检测维C银翘片中的对乙酰氨基酚[J].中国药师,2011,14(8):1145-1147.
    [6] 吴 翔,韩 莹.应用近红外光谱法快速检测药品白加黑真伪的研究[J].北方药学,2011,8(7):10-11.
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Study on the identification of raceanisodamine tablets by near infrared spectroscopy

doi: 10.3969/j.issn.1006-0111.2014.05.011
  • 1. Department of Pharmacy, First Affiliated Hospital, General Hospital of PLA, Beijing 100048, China
  • 2. Qinghai Institute for Drug Control, Xining 810016, China
  • Received Date: 2013-12-30
  • Rev Recd Date: 2013-10-29

Abstract: Objective To develop an identification model of raceanisodamine tablets by diffuse reflection near-infrared spectroscopy and pattern recognition. Methods The diffuse reflectance spectra in the 12 000-4 000 cm-1 spectral coverage range of raceanisodamine tablets from eight different pharmaceutical factories were collected to establish the identification model.A mono-component near infrared model was established for raceanisodamine tablets. Results The parameters of the identification model for the raceanisodamine tablets was as follows:spectral range was 5 400-7 000 cm-1, the pretreatment method was first derivative and normalization; the threshold was 0.603. And the model was validated, which met the requirements of application. Conclusion The results showed that identification model for the raceanisodamine tablets by near infrared spectroscopy was feasible, which provided a reference method for the model updating.

WANG Chongqing, MA Ningning, YANG Chao, LIU Shihao, ZHU Ju, ZHENG Canhui. Research progress in the catalytic rearrangement reaction of benzyl phenyl ethers[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(6): 486-489. doi: 10.3969/j.issn.1006-0111.2015.06.002
Citation: JIA Yanhua, XIONG Chengwen. Study on the identification of raceanisodamine tablets by near infrared spectroscopy[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(5): 357-359. doi: 10.3969/j.issn.1006-0111.2014.05.011
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