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Volume 25 Issue 6
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2007  >  (6): 391-391

ZHANG Mei-ling. Content determination of aconitine in Shangke liniment by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2007, (6): 391-391.
Citation: ZHANG Mei-ling. Content determination of aconitine in Shangke liniment by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2007, (6): 391-391.
shu

Content determination of aconitine in Shangke liniment by HPLC

  • Department of Pharmacy,Tongde Hospital of Zhejiang Province,Hangzhou310012,China

  • Received Date: 2006-05-08
  • Objective :To set up an HPLC method for the content determination of aconitine in shangke liniment. Methods :Chromatography was performed on a MN-Nucleosil 7C6H5 stainless steel column（25 cm×4.0 mm）.The mobile phase was a mixture of methanol-water-chloroform-triethylamine（70-30-1-0.2）,with a flow rate of 1.5 mL/min.The detection wavelength was 235 nm. Results :The calibration curve was linear over the range of 0.050-0.225 μg,the average rate of recovery was 95.42 %,RSD=1.62 %（n=5）. Conclusion :The method proved to be simple,rapid,reliable and well reproducible in the content determination of aconitine in shangke liniment.It may be used as a method of quality control of the preparation.
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Content determination of aconitine in Shangke liniment by HPLC

  • Department of Pharmacy,Tongde Hospital of Zhejiang Province,Hangzhou310012,China
  • Received Date: 2006-05-08

Abstract: Objective :To set up an HPLC method for the content determination of aconitine in shangke liniment. Methods :Chromatography was performed on a MN-Nucleosil 7C6H5 stainless steel column（25 cm×4.0 mm）.The mobile phase was a mixture of methanol-water-chloroform-triethylamine（70-30-1-0.2）,with a flow rate of 1.5 mL/min.The detection wavelength was 235 nm. Results :The calibration curve was linear over the range of 0.050-0.225 μg,the average rate of recovery was 95.42 %,RSD=1.62 %（n=5）. Conclusion :The method proved to be simple,rapid,reliable and well reproducible in the content determination of aconitine in shangke liniment.It may be used as a method of quality control of the preparation.

ZHANG Mei-ling. Content determination of aconitine in Shangke liniment by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2007, (6): 391-391.
Citation: ZHANG Mei-ling. Content determination of aconitine in Shangke liniment by HPLC[J]. Journal of Pharmaceutical Practice and Service, 2007, (6): 391-391.
shu

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