白蔹的化学成分研究
Chemical constituents of Ampelopsis japonica(Thunb.) Makino
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摘要: 目的 研究白蔹的化学成分。 方法 利用各种色谱法进行分离,根据理化性质和波谱分析鉴定化合物结构。 结果 从白蔹的氯仿和乙酸乙酯萃取部分又分离得到7个已知成分,分别鉴定为甲基-α-D-呋喃果糖苷(1)、甲基-β-D-吡喃果糖苷(2)、β-D-呋喃果糖甲苷(3)、β-D-呋喃果糖(4)、尿苷(5)、腺苷(6)、大黄素-8-O-β-D-吡喃葡萄糖苷(7)。 结论 化合物1、2、3、4、5、6为首次从该植物中分离得到。Abstract: Objective To isolate and identify the compounds from the Ampelopsis japonica(Thunb.) Makino. Methods The compounds were separated and purified by column chromatography and their structures were established by spectroscopic methods. Results Seven compounds were obtained from the chloroform and ethyl acetate extracts of the Ampelopsis japonica(Thunb.) Makino which were determined as Methyl-α-D-frucofuranoside (1), Methyl-β-D-frucofuranoside (2), Methyl-β-D-frucopyranoside (3),Methyl-β-D-frucofuranose(4),Uridine(5),Adenosine(6),Emodin-8-O-β-D-glucopyranoside (7). Conclusion Compounds 1,2,3,4,5,6 were isolated from the Ampelopsis japonica(Thunb.) Makino for the first time.
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[1] 郭启雷,杨峻山,刘建勋,等. 羊耳菊的化学成分研究[J].中成药,2007,6(29):887. [2] Stephen JA,Geoffrey SB. Conformational analysis in carbohydrate chemistry.Ⅲ* The 13C-NMR spectra of the hexuloses[J].Aust J Chem,1976,29(3):1249. [3] HU XY,DOU DQ,PEI YP.Chemical Constituents of Roots of Ranunculus terna tus Thunb[J].J chi Phar Sci,2006, 15 (2):127. [4] 白 冰,刘绣华,王 勇,等. 怀山药化学成分研究(Ⅱ)[J].化学研究,2008,19(3):67. [5] 邬秋萍,王祝举,付梅红,等.番泻叶的化学成分研究[J]. 中药材,2007,30(10):1250. -
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