康肾丸质量控制的研究
Studies on quality control of Kangshen pills
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摘要: 目的: 建立康肾丸的质量控制方法。 方法: 采用薄层色谱法(TLC)对方中主要药材黄芪、虫草菌丝粉、防风分别进行定性鉴别;采用高效液相色谱法(HPLC)测定黄芪甲苷的含量。 结果: 定性鉴别方法重现性好,专属性强;含量测定的加样回收率为99.39%,RSD为0.59%。 结论: 本方法简单、易行、精密度高、重复性好,能够有效地控制康肾丸的质量。Abstract: Objective: To establish a method for quality control of Kangshen pills. Methods: The qualitative analysis of Radix As- tragali,mycelium powder of Cordyceps Sinrnsis,Radix Saposhnikoviae in Kangshen pills were identified by TLC.The content of astra- galosideⅣwas determinated by HPLC. Results: Methods of the qualitative identification were specific and reproducible.The average recovery was 99.39% and relative standard deviation was 0.59%. Conclusion: The precision and reproducibility of the method were good.The method can be used for quality control of Kangshen pills.
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Key words:
- Kangshen pill /
- TLC /
- astragalosideⅣ /
- HPLC
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