Identification of different breeds of Fagopyrum tataricum by differential thermal analysis and near infrared reflectance spectroscopy
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摘要: 目的 用差热分析法(DTA)和近红外漫反射光谱(NIRS)法对11种栽培苦荞麦进行快速分析鉴别。 方法 应用TG-DTA热重差热联用仪分别对11个栽培品种苦荞麦进行差热图谱扫描与分析。实验条件为差热量程:±50 μV;升温速率:15 ℃/min;升温范围:35 ℃~500 ℃;气氛为氮气,流速:50 ml/min。应用Bruker Vector 22/N 型傅立叶变换近红外光谱仪对11种栽培苦荞麦进行扫描。实验条件为测定方式:积分球漫反射;扫描次数64次;扫描范围:3 700~12 000/ cm。 结果
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关键词:
- 苦荞麦 /
- 差热分析(DTA) /
- 近红外漫反射光谱(NIRS) /
- 鉴别
Abstract: Objective To identify different breeds of Fagopyrum tataricum by differential thermal analysis and near infrared reflectance spectroscopy. Methods TG/DTA and thermal analysis were both used to scan and analyze the thermal map of 11 breeds of F. tartaricum. The experiment conditions included DTA range of ±50 μV, a calefactive rate of 15 ℃/min, an ambience of nitrogen and flow velocity of 50 ml/min. Bruker Vector 22/N-type Fourier transform near infrared spectroscopy was used to scan and analyze of 11 breeds F. tartaricum. Experiment conditions were: integrating sphere diffuse reflectance as measure methods; scan for 64 times; 3 700 ~ 12 000/cm as scan range. Results Both methods could identify the Jiande tartary buckwheat from other breeds. Conclusion Jiande tartary buckwheat was a new cultivar, nutrient value and pharmacological activity of which should be evaluated for promotion. -
[1] 胡一冰,杨敬东,邹 亮,等.苦荞麦药理研究及临床应用概况[J]. 成都大学学报(自然科学版), 2006,25(4): 271. [2] 田秀红,任 涛. 苦荞麦的营养保健作用与开发利用[J].中国食物与营养, 2007,(10): 44. [3] 田秀红,刘鑫峰,闫 峰,等.苦荞麦的药理作用与食疗[J].农产品加工·学刊,2008,(8):31. [4] 朱 瑞,高南南,陈建民.苦荞麦的化学成分和药理作用[J].中国野生植物资源,2003,(4):7. [5] 刘三才,李为善,刘 方,等.苦荞麦种质资源总黄酮和蛋白质含量的测定与评价[J].植物遗传资源学报,2007,8(3):317. [6] 程存归,刘幸海.差热分析法鉴定贝母类中药材的研究[J].中草药,2004,35(2):210. [7] Ghosh S, Rodgers J. Handbook of near-infrared analysis, practical spectroscopy Series[M]. New York:Marcel Dekker Inc,1992: 495. [8] 龚海燕,白 雁,宋瑞丽,等.近红外光谱结合聚类分析鉴别铁棍山药和白玉山药[J].中国医院药学杂志,2010,30(9):735. [9] 张延莹,张金巍,刘 岩.近红外光谱技术鉴别三七及其伪品[J].中药材,2010,3:364. [10] 林 兵,胡长玲,黄 芳,等.苦荞麦的化学成分和药理活性研究进展[J].现代药物与临床,2011,26(1):29. [11] 韩 丹,王晓丹,陈 霞,等.苦荞麦制麦芽及其啤酒发酵工艺研究[J].食品与机械,2010(1): 125. [12] 花旭斌,李正涛, 张 忠,等.苦荞麦叶片制茶工艺的探讨[J].西昌学院学报:社会科学版,2004(4):126. [13] 张怀珠,王立军,彭 涛.无糖苦荞苏打饼干的工艺研究[J].食品工业,2010,(1):77. [14] Kim SL,Kim SK,Park CH.Introduction and nutritional evaluation of buckwheat sprouts as a new vegetable[J]. Food Res Int, 2004,37(4): 319. [15] 龚 丽,胡光华,毛 新,等.膨化苦荞麦茶泡茶特性研究[J].食品科技,2011,36(5):117. -
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