HPLC法测定乳癖消片中芍药苷含量
Determination of paecniflorin in Rupixiao tablets by HPLC
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摘要: 目的:建立HPLC法测定乳癖消片中芍药苷含量的方法。方法:采用Diamonsil C18色谱柱,乙腈-水(20:80)为流动相,流速1.0 mL/min,检测波长为230 nm。结果:芍药苷线性范围为4.0-16.0μg/mL,平均回收率为99.75%,RSD为1.07%。结论:该方法简便、可靠、准确,可用于该制剂的质量控制。Abstract: Objective :To establish a method of HPLC for determination of paecniflorin in Rupixiao tablets. Methods :A Diamonsil C18 column was used.The mobile phase was acetonitrile-water(20∶80).The flow rate was 1.0 mL/min.The detection wavelength was set as 230 nm. Results :The linear range of paecniflorin was 4.0~16.0 μg/mL,and the average recovery rate was 99.75%,RSD was 1.07%. Conclusion :The method is simple,reliable,and accurate and can be applied to the quality control of preparation.
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Key words:
- Rupixiao tablet /
- paecniflorin /
- HPLC
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