2007 Vol. 25, No. 5
Display Method:
2007, (5): 290-291.
Abstract:
Objective : To determine the dissociation constant and partition coefficient of mesylate delavirdine. Methods :The dissociation constant was determined with acid-base titration method in methanol /water solutions with different ratios,the value to in...
Objective : To determine the dissociation constant and partition coefficient of mesylate delavirdine. Methods :The dissociation constant was determined with acid-base titration method in methanol /water solutions with different ratios,the value to in...
2007, (5): 292-294.
Abstract:
Objective :To modify a patent method concerning determination of synthetic drugs in traditional chinese medicines based on infrared spectroscopy,in order to improve the accuracy of judgment. Methods : The influences of two different derivative method...
Objective :To modify a patent method concerning determination of synthetic drugs in traditional chinese medicines based on infrared spectroscopy,in order to improve the accuracy of judgment. Methods : The influences of two different derivative method...
2007, (5): 295-296,302.
Abstract:
Objective :To study the angiogenesis effects of Shexiang Baoxin pill on cancer. Methods :The model of liver metastasis of colorectal cancer was established on 40 BALB/C nude mice which were xenotransplanted through intraspleen injection of LoVo cells...
Objective :To study the angiogenesis effects of Shexiang Baoxin pill on cancer. Methods :The model of liver metastasis of colorectal cancer was established on 40 BALB/C nude mice which were xenotransplanted through intraspleen injection of LoVo cells...
2007, (5): 297-299.
Abstract:
Objective :To evaluate the clinical efficacy between urapidil and other vasodilators in acute left heart failure. Methods : 80 patients with acute left heart failure were randomly divided into 4 groups: urapidil group(n=19),phentolamine group(n=21),s...
Objective :To evaluate the clinical efficacy between urapidil and other vasodilators in acute left heart failure. Methods : 80 patients with acute left heart failure were randomly divided into 4 groups: urapidil group(n=19),phentolamine group(n=21),s...
2007, (5): 300-302.
Abstract:
Objective :To establish by capillary gas chromatography for the analysis of organic residual in olmesartan medoxomil by direct injection of solution,and compare with the results. Methods :Wide-bore capillary column(30m ×0.53mm) packed with 6% cyanopr...
Objective :To establish by capillary gas chromatography for the analysis of organic residual in olmesartan medoxomil by direct injection of solution,and compare with the results. Methods :Wide-bore capillary column(30m ×0.53mm) packed with 6% cyanopr...
2007, (5): 303-306.
Abstract:
Objective :To synthesize metallic salts of norfloxacin(NFLO) and evaluate their bacteriaostatic activities in vitro. Methods : The compounds were syntherized from the starting material norfloxacin and metallic salts.The bateriostatic activities of th...
Objective :To synthesize metallic salts of norfloxacin(NFLO) and evaluate their bacteriaostatic activities in vitro. Methods : The compounds were syntherized from the starting material norfloxacin and metallic salts.The bateriostatic activities of th...
2007, (5): 307-309.
Abstract:
Objective : To establish an HPLC method for determination of salvianolic acid B in Danshen leaves and stems,and compare the content of salvianolic acid B in Danshen leaves and stems of different species,different locations and growth stages,so as to ...
Objective : To establish an HPLC method for determination of salvianolic acid B in Danshen leaves and stems,and compare the content of salvianolic acid B in Danshen leaves and stems of different species,different locations and growth stages,so as to ...
2007, (5): 310-312.
Abstract:
Objective :To study the synthesis of finasteride. Methods : Finasteride was synthesized from pregnenolone acetic ester,and by hypobromous acid oxidation,methanol esterification to give 3-oxo-4-androstene-17β-carboxylic methyl ester.Then by Oppenauer ...
Objective :To study the synthesis of finasteride. Methods : Finasteride was synthesized from pregnenolone acetic ester,and by hypobromous acid oxidation,methanol esterification to give 3-oxo-4-androstene-17β-carboxylic methyl ester.Then by Oppenauer ...
2007, (5): 312-314,345.
Abstract:
Objective : To improve the synthetic process of 7-azaindol-3-carboxylic acid. Methods : The succinonitrile was taken as the original raw material.The isopropyl ether,n-heptane,and chlorobenzene, which were used in original technics,were subsituted by...
Objective : To improve the synthetic process of 7-azaindol-3-carboxylic acid. Methods : The succinonitrile was taken as the original raw material.The isopropyl ether,n-heptane,and chlorobenzene, which were used in original technics,were subsituted by...
2007, (5): 325-327.
Abstract:
Objective :To discuss the feasibility of determining the contents of trace element in Fructus cnidii by spectrophotometry,and to expound the potential relationship between the sorts and contents of the elements in crude drugs and the pharmacological ...
Objective :To discuss the feasibility of determining the contents of trace element in Fructus cnidii by spectrophotometry,and to expound the potential relationship between the sorts and contents of the elements in crude drugs and the pharmacological ...
2007, (5): 328-330.
Abstract:
Objective :To establish a method for the determination of the content of procaine hydrochloride in cradiac standstill solution. Method:Ultraviolet spectrophotometric method was used to directly determine the content of procaine hydrochloride.The wave...
Objective :To establish a method for the determination of the content of procaine hydrochloride in cradiac standstill solution. Method:Ultraviolet spectrophotometric method was used to directly determine the content of procaine hydrochloride.The wave...
2007, (5): 330-331,333.
Abstract:
Objective :To establish a method of HPLC for determination of paecniflorin in Rupixiao tablets. Methods :A Diamonsil C18 column was used.The mobile phase was acetonitrile-water(20∶80).The flow rate was 1.0 mL/min.The detection wavelength was set as 2...
Objective :To establish a method of HPLC for determination of paecniflorin in Rupixiao tablets. Methods :A Diamonsil C18 column was used.The mobile phase was acetonitrile-water(20∶80).The flow rate was 1.0 mL/min.The detection wavelength was set as 2...
2007, (5): 332-333.
Abstract:
Objective :To establish a method for determining the content of hydroquinone in compound hydroquinone cream. Methods :The dual wavelength UV-spectrophotometric method was used for hydroquinone analysis. Results :The linear range of hydroquinone was 4...
Objective :To establish a method for determining the content of hydroquinone in compound hydroquinone cream. Methods :The dual wavelength UV-spectrophotometric method was used for hydroquinone analysis. Results :The linear range of hydroquinone was 4...
2007, (5): 334-336.
Abstract:
Objective :To establish the determination method of the content of psoralen and isopsoralen in compound Buguzhi granule. Methods :A HPLC method was adopted.This analysis was carried on a column of Waters RP-C18 with a mobile phase of water-methanol a...
Objective :To establish the determination method of the content of psoralen and isopsoralen in compound Buguzhi granule. Methods :A HPLC method was adopted.This analysis was carried on a column of Waters RP-C18 with a mobile phase of water-methanol a...
2007, (5): 340-342,345.
Abstract:
Objective : To discuss the current status and the developing direction of Chinese traditional drug pharmacovigilance. Methods : Comparing with the advanced work of the pharmacovigilance in the world.The instruction books,the expression of Chinese tra...
Objective : To discuss the current status and the developing direction of Chinese traditional drug pharmacovigilance. Methods : Comparing with the advanced work of the pharmacovigilance in the world.The instruction books,the expression of Chinese tra...
2007, (5): 346-347,352.
Abstract:
Objective :To provide references for the rational use of dl-lysine acetylsalicylate in clinical practice. Methods :Adverse reactions resulted from dl-lysine acetylsalicylate reported in recent years in domestic literatures were statistically classifi...
Objective :To provide references for the rational use of dl-lysine acetylsalicylate in clinical practice. Methods :Adverse reactions resulted from dl-lysine acetylsalicylate reported in recent years in domestic literatures were statistically classifi...
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